Certyfikat Nr 17/2017/DPL


Physicochemical studies, residue studies, biodegradation studies, efficacy studies of biocides:
- Statement of GLP compliance No 17/2017/GLP.

 

Determination of physical, chemical and technical properties of substances and chemical products

Normative documents / own method

 1

Relative density of liquids and solids

OECD 109; ISO649/1-2:1981;
ISO 758:1976; ISO 35-07:1999; ISO 901:1976; ISO 787-10:1993;

PN-C-0504: 1982,

CIPAC MT 3/ EEC A3

2

Determination of pH values

PN-C-04665:2001

i CIPAC MT 75

3

Free acidity or alkalinity

PN-C-04665:2001

i CIPAC MT 31

4

Kinematic and dynamic viscosity of Newtonian liquids

OECD 114;
PN-EN ISO 3105: 2002,

5

Viscosity of Newtonian and non - Newtonian fluids

PN-EN-ISO 3219:2000

PN-EN12092: 2004

6

Determination of Weight Loss of Tested Material

CIPAC MT 17

7

Ambient temperature storage procedure

Technical Monograph
GIFAP No 17

8

Accelerated storage procedure

CIPAC MT 46

9

Low temperature (0°C) storage procedure

CIPAC MT 39

10

Low temperature (0°C) stability testing of liquids

CIPAC MT 39

11 

Dilution stability

CIPAC MT 41

CIPAC MT 179

12

Pourability of suspension concentrates

CIPAC MT 148

13

Wettability

PN-C-04662:1987;

 CIPAC MT 53.3

14

Suspensibility

CIPAC MT 15.1; CIPAC MT 161;
CIPAC MT 168;  MT 184

15

Emulsifiability, re-emulsifiability and emulsion stability, dispersion stability

PN-C-04652:1998; 
CIPAC MT 36; CIPAC MT 173; CIPAC MT 180

16

Persistent foaming

CIPAC MT 47

17

Tap density

CIPAC MT 33, CIPAC MT 159, CIPAC MT 169, CIPAC MT 186 

18

Dry sieve test

CIPAC MT 59.1

CIPAC MT 58.2

19

Wet sieve test

CIPAC MT 59.3,

CIPAC MT 167,
iCIPAC MT 185,

20

Dissolution rate of water soluble bags

CIPAC MT 176

21

Packaging stability

Technical Monograph
GIFAP  No 17

22

Pourability and effectiveness of cleaning procedures

Own method

23

Appearance

OPPTS 830.6302 to 04

24

Determination of particle size distribution by Laser difraction

CIPAC MT 187

ISO 13320-1:1999

25

Determination of the Spontaneity Dispersion of Suspension Concentrates

 CIPAC MT 160,

  CIPAC MT 174

26

Determination of Granular Product Dust Content

CIPAC MT 171.

27

Determination of pesticides solubility rate

CIPAC MT 60

28

Determination of seed to seed uniformity of distribution for liquid seed-treatment formulations

CIPAC MT 175

29

Flowability of granules

CIPAC MT 172

 

30

Friability  resistence test

CIPAC MT 58.2

31

Determination of aerosol discharge rate

Manual on development, Revised First Edition, March 2006

32

Determination of spray diameter

Manual on development, Revised First Edition, March 2006

33

Surface tension

OECD 115/ EEC A.5

34

 Water solubility

OECD 105/ EEC A6

35

Partition coefficient (n-octanol/water): shake flask method

OECD 107 /EEC A.8

36

Partition Coefficient (n-octanol/water), HPLC Method

OECD 117

37

 Partition coefficient (n-octanol/water), slow stirring method

OECD 123

38

 Partition coefficient (n-octanol/water), pH-metric method for ionisable substances

OECD 122

39

Melting temperature

OECD 102/ EEC A1

40

Crystallization temperature

PN ISO 1392:2002

OECD 102

41

Boiling temperature

OECD 103/EEC A2

42

Hydrolysis as a function of pH

OECD 111/EEC C.7

43

Dissociation constants in water

OECD 112

44

Phototransformation of chemicals in water - direct and indirect photolysis

OECD 316

45

Photodegradation of chemical substances on soil

OPPTS 835.2410

46

Thermal stability of chemical substances in air

OECD 113

47

Refraction index determination

Farmakopea Poland wyd. VI 2002

48

Determination of optical  rotation of chemical substances

Farmakopea Poland wyd. VI 2002

49

Accelerated ageing test of chemical substances and the mixtures of them at 400C and 75% relative  humidity

According to no 75/318/EEC directive, app. ICH Q1A

50

Long term Accelerated ageing test of chemical substances and the mixtures of them at 250C and 60 % relative  humidity

According to no 75/318/EEC directive, app. ICH Q1A

51

 Vapor pressures

OECD 104 / EEC A.4

52

 Oxidizing properties  (solids)

EEC A.17

53

  Pyrophoric properties of solids and liquids

EEC A.13

54

 Oxidizing properties ( liquids)

EEC A.21

55

 Auto-ignition temperature (liquids)

EEC A.15

56

 Minimum ignition temperatures of dust

PN-EN 50281-2-1:2002

57

Flammability solids

EEC A.10

58

Flash point

EEC A.9

59

 Ability of solids to self-heating up to self-ignition

Test UN N.4

60

 Initial boiling point

PN-ISO 918:2000

ASTM D86-09

PN-EN ISO 3405:2012

61

 Relative self-ignition temperature for solids

EEC A.16

62

Explosive properties

  • §impact sensitivity
  • §friction sensitivity
  • §thermal sensitivity

 

EEC A.14


 

Mr Maciej Sliwakowski, PhD
Head, Analytical Department
kielczewska@ipo.waw.pl
phone (+48) 22 603 555 632
fax (+48) 22 811 07 99


Head of Chemical Safety and Static Electricity Department
Michał Frączak, MSc
Tel. (+48 22) 811 12 31 ext. 350
fraczak@ipo.waw.pl
 
Pesticides Application Dept.
Idris Ahmed Al Amin, PhD. Eng.
Tel. (+48 22) 811 12 31 ext. 225
zielinski@ipo.waw.pl

Active Ingredients Synthesis and Technology Dept.
Jerzy Zakrzewski, PhD. Eng.
Tel. (+48 22) 811 12 31 ext. 316, 331
zakrzewski@ipo.waw.pl